MO ASP Metals by EPA 6020A EPA 6020A EPA 6020A EPA 6020A EPA 6020A EPA 6020A EPA 6020A EPA 6020A EPA 6020A EPA 6020A EPA 6020A EPA 6020A EPA 6020A EPA 6020A EPA 6020A EPA 6020A EPA 6020A Aluminum Antimony Arsenic Barium Beryllium Cadmium Chromium Cobalt Copper Lead Manganese Nickel Selenium Silver Thallium Vanadium 38.0 < LOQ < LOQ 339 < LOQ < LOQ < LOQ 29.9 < LOQ < LOQ 1150 197 < LOQ < LOQ < LOQ < LOQ J NYSDOH ELAP and NELAC do not offer accreditation for Alkalinity, Ammonia, Biochemical Oxygen Demand, Total Kjeldahl Nitrogen and Total Phosphorus in the S&HW Matrix. Unless the sample is otherwise qualified, all Quality Control acceptance criteria have satisfied method and NELAC requirements. DL = Detection Limit Approved By LOQ = Limit of Quantitation Robert Hilbrandt Environmental Laboratories NYS ELAP # 10108 (914) 231-1620 J=value is an estimate QA Officer Report Number: H = exceeds holding time Date Approved : 1772 07/12/2021 EMAIL 7/12/2021 These analytical results relate only to the sample identified in this report. Page 1 of 4 AX08484 Sample No. Method Test Description EPA 6020A Results Zinc Qualifier Units < LOQ DL/LOQ Analyzed on ug/L Validator 80.0 05/19/2021 MO "J" Flag - Estimated value for Aluminum found below the calibration range and at or above the detection limit. RWHJr SM22 2320B Alkalinity as Calcium Carbonate - ASP >500 mg/L 5.0 05/07/2021 MO Alaklinity result beyond titrametric range of instrument, upper limit reported SM22-5210B Biochemical Oxygen Demand ASP BOD Set Date and Time EPA 6010C ASP Calcium by ICP-AES SW846/9253 Chloride - ASP SW846-9012A ASP Total Cyanide HACH 8000 Chemical Oxygen Demand - ASP SM20-2120B Color, Apparent - ASP EPA 6010C ASP Hardness as Calcium Carbonate SW846-7196A Hexavalent Chromium, ASP SW846-7470A ASP Mercury SW846-6010C ASP Magnesium SM22-4500NH3-G Ammonia as N SM22-4500NO2B Nitrite Nitrogen as N EPA 353.2, Rev 2.0 N-Nitrate Calculated EPA 9040C Corrosivity/pH SM21-5210B < LOQ Completed 84900 90.0 < LOQ 76 75 450 < LOQ < LOQ 57400 < LOQ < LOQ < LOQ 7.22 mg/L ug/L mg/L mg/L mg/L units mg/L ug/L ug/L ug/L mg/L mg/L mg/L Units 2 05/10/2021 9:53 am 05/05/2021 11:32 am 1000 05/20/2021 25.0 05/25/2021 0.005 05/12/2021 5.0 05/10/2021 5 05/04/2021 2:56 pm 1 05/21/2021 40 05/04/2021 3:06 pm 0.20 05/14/2021 1000 05/20/2021 0.05 05/21/2021 0.01 05/05/2021 11:23 am 0.05 05/21/2021 0.1 05/04/2021 2:56 pm Note: The Corrosivity/pH test is an Analyze Immediately On-Site (AIOS) parameter. AIOS parameters have a 15 minute hold time. The Laboratory provides this test result only as a guide. RWHJr EPA 9065 Phenolics, Total Recoverable Not Detected mg/L 0.004 05/13/2021 SW846-3005A ASP Metals Digestion - Aqueous Completed 05/13/2021 40CFR136 NH4 Preparation Completed 05/20/2021 Ammonia as N analyzed by On-line Gas Diffusion Automated Salicylate Method, as appears in Method Update Rule II, 40CFR 136, Table 1B, Federal Register Volume 77 Number 97, pursuant to Clean Water Act promulgated 06/01/2012. 40CFR136 SW846/9056A SM22-2540C SM22-4500Norg D SW846-9060A EPA 180.1 TKN Digestion/Diffusion Method Sulfate, Aqueous - ASP Total Dissolved Solids Total kjeldahl nitrogen as N - ASP Total Organic Carbon - ASP Turbidity Completed 13.3 720.0 0.443 28.6 198 05/24/2021 1.0 05/14/2021 2.0 05/05/2021 0.06 05/26/2021 0.25 05/20/2021 0.2 05/04/2021 mg/L mg/L mg/L mg/L as C NTU 2:56 pm MO MO MO MO MO MO JLM MO MO MO MO MO MO MO JLM MO MO RH MO MO MO MO MO JLM Organics VOCs by 8260C Baseline Expanded SW846 8260C 1,2-dibromo-3-chloropropane < LOQ ug/L 0.500 05/13/2021 MG SW846 8260C 1,2-dibromoethane < LOQ ug/L 0.500 05/13/2021 MG SW846 8260C 2-hexanone < LOQ ug/L 5.00 05/13/2021 MG SW846 8260C Acetone < LOQ ug/L 10.0 05/13/2021 MG SW846 8260C Acetonitrile < LOQ ug/L 50.0 05/13/2021 MG SW846 8260C Acrolein < LOQ ug/L 5.00 05/13/2021 MG SW846 8260C Acrylonitrile < LOQ ug/L 5.00 05/13/2021 MG NYSDOH ELAP and NELAC do not offer accreditation for Alkalinity, Ammonia, Biochemical Oxygen Demand, Total Kjeldahl Nitrogen and Total Phosphorus in the S&HW Matrix. Unless the sample is otherwise qualified, all Quality Control acceptance criteria have satisfied method and NELAC requirements. DL = Detection Limit Approved By LOQ = Limit of Quantitation Robert Hilbrandt Environmental Laboratories NYS ELAP # 10108 (914) 231-1620 J=value is an estimate QA Officer Report Number: H = exceeds holding time Date Approved : 1772 07/12/2021 EMAIL 7/12/2021 These analytical results relate only to the sample identified in this report. Page 2 of 4 AX08484 Sample No. Method Test Description Results Qualifier Units DL/LOQ Analyzed on Validator SW846 8260C Carbon Disulfide < LOQ ug/L 5.00 05/13/2021 MG SW846 8260C Methyl Iodide < LOQ ug/L 5.00 05/13/2021 MG SW846 8260C Prep. Method 5030C ug/L 05/13/2021 MG SW846 8260C trans-1,4-dichloro-2-butene < LOQ ug/L 5.00 05/13/2021 MG SW846 8260C Vinyl Acetate < LOQ ug/L 5.00 05/13/2021 MG The following tentatively identified compound (TIC) is present; the concentration