as appears in Method Update Rule II, 40CFR 136, Table 1B, Federal Register Volume 77 Number 97, pursuant to Clean Water Act promulgated 06/01/2012. 40CFR136 SW846/9056A SM22-2540C SM22-4500Norg D SW846-9060A EPA 180.1 TKN Digestion/Diffusion Method Sulfate, Aqueous - ASP Total Dissolved Solids Total kjeldahl nitrogen as N - ASP Total Organic Carbon - ASP Turbidity Completed 29.2 606.7 0.917 2.54 195 05/24/2021 1.0 05/14/2021 2.0 05/05/2021 0.06 05/26/2021 0.25 05/20/2021 0.2 05/04/2021 mg/L mg/L mg/L mg/L as C NTU 2:56 pm MO MO MO MO MO MO JLM MO MO MO MO MO MO MO JLM MO MO RH MO MO MO MO MO JLM Organics VOCs by 8260C Baseline Expanded SW846 8260C 1,2-dibromo-3-chloropropane < LOQ ug/L 0.500 05/13/2021 MG SW846 8260C 1,2-dibromoethane < LOQ ug/L 0.500 05/13/2021 MG SW846 8260C 2-hexanone < LOQ ug/L 5.00 05/13/2021 MG SW846 8260C Acetone < LOQ ug/L 10.0 05/13/2021 MG SW846 8260C Acetonitrile < LOQ ug/L 50.0 05/13/2021 MG SW846 8260C Acrolein < LOQ ug/L 5.00 05/13/2021 MG SW846 8260C Acrylonitrile < LOQ ug/L 5.00 05/13/2021 MG NYSDOH ELAP and NELAC do not offer accreditation for Alkalinity, Ammonia, Biochemical Oxygen Demand, Total Kjeldahl Nitrogen and Total Phosphorus in the S&HW Matrix. Unless the sample is otherwise qualified, all Quality Control acceptance criteria have satisfied method and NELAC requirements. DL = Detection Limit Approved By LOQ = Limit of Quantitation Robert Hilbrandt Environmental Laboratories NYS ELAP # 10108 (914) 231-1620 J=value is an estimate QA Officer Report Number: H = exceeds holding time Date Approved : 1772 07/12/2021 EMAIL 7/12/2021 These analytical results relate only to the sample identified in this report. Page 2 of 4 AX08486 Sample No. Method Test Description Results Qualifier Units DL/LOQ Analyzed on Validator SW846 8260C Carbon Disulfide < LOQ ug/L 5.00 05/13/2021 MG SW846 8260C Methyl Iodide < LOQ ug/L 5.00 05/13/2021 MG SW846 8260C Prep. Method 5030C ug/L 05/13/2021 MG SW846 8260C trans-1,4-dichloro-2-butene < LOQ ug/L 5.00 05/13/2021 MG SW846 8260C Vinyl Acetate < LOQ ug/L 5.00 05/13/2021 MG The following tentatively identified compounds (TIC) are present; the concentrations given are estimates: Difluorochloromethane 8.75 ug/L Choroethene 10.7 ug/L Fluorodichloromethane 7.23 ug/L Ethyl ether 16.2 ug/L (E)-1,2-dichloro-Ethylene 23.4 ug/L MG 6/28/21 Tentative identification of non-target sample components has to have an area height >10% nearest internal standard and a mass spectral library search result (Q-value) of 85% or greater for reporting. The laboratory provides these TIC results to facilitate remediation. NYSDOH ELAP and NELAC do not offer accreditation for these TIC list chemicals in the S&HW matrix. RWHJr VOC's in water-EPA 8260C SW846 8260C 1,1,1- trichloroethane < LOQ ug/L 0.50 05/18/2021 MG SW846 8260C 1,1,1,2-tetrachloroethane < LOQ ug/L 0.50 05/18/2021 MG SW846 8260C 1,1,2,2-tetrachloroethane < LOQ ug/L 0.50 05/18/2021 MG SW846 8260C 1,1,2-trichloroethane < LOQ ug/L 0.50 05/18/2021 MG SW846 8260C 1,1-dichloroethane 7.28 ug/L 0.50 05/18/2021 MG SW846 8260C 1,1-Dichloroethene < LOQ ug/L 0.50 05/18/2021 MG SW846 8260C 1,1-dichloropropene < LOQ ug/L 0.50 05/18/2021 MG SW846 8260C 1,2,3-trichlorobenzene < LOQ ug/L 0.50 05/18/2021 MG SW846 8260C 1,2,3-trichloropropane < LOQ ug/L 0.50 05/18/2021 MG SW846 8260C 1,2,4-trichlorobenzene < LOQ ug/L 0.50 05/18/2021 MG SW846 8260C 1,2,4-trimethylbenzene < LOQ ug/L 0.50 05/18/2021 MG SW846 8260C 1,2-dichlorobenzene < LOQ ug/L 0.50 05/18/2021 MG SW846 8260C 1,2-dichloroethane 1.05 ug/L 0.50 05/18/2021 MG SW846 8260C 1,2-dichloropropane 0.450 ug/L 0.50 05/18/2021 MG SW846 8260C 1,3,5-trimethylbenzene < LOQ ug/L 0.50 05/18/2021 MG SW846 8260C 1,3-dichlorobenzene < LOQ ug/L 0.50 05/18/2021 MG SW846 8260C 1,3-dichloropropane < LOQ ug/L 0.50 05/18/2021 MG SW846 8260C 1,4-dichlorobenzene < LOQ ug/L 0.50 05/18/2021 MG SW846 8260C 2,2-dichloropropane < LOQ ug/L 0.50 05/18/2021 MG SW846 8260C 2-butanone (MEK) < LOQ ug/L 2.00 05/18/2021 MG SW846 8260C 2-chlorotoluene < LOQ ug/L 0.50 05/18/2021 MG SW846 8260C 4-chlorotoluene < LOQ ug/L 0.50 05/18/2021 MG SW846 8260C Benzene < LOQ ug/L 0.50 05/18/2021 MG SW846 8260C Bromobenzene < LOQ ug/L 0.50 05/18/2021 MG SW846 8260C Bromochloromethane < LOQ ug/L 0.50 05/18/2021 MG SW846 8260C Bromodichloromethane < LOQ ug/L 0.50 05/18/2021 MG J NYSDOH ELAP and NELAC do not offer accreditation for Alkalinity, Ammonia, Biochemical Oxygen Demand, Total Kjeldahl Nitrogen and Total Phosphorus in the S&HW Matrix. Unless the sample is otherwise qualified, all Quality Control acceptance criteria have satisfied method and NELAC requirements. DL = Detection Limit Approved By LOQ = Limit of Quantitation Robert Hilbrandt Environmental Laboratories NYS ELAP # 10108 (914) 231-1620 J=value is an estimate QA Officer Report Number: H = exceeds holding time Date Approved : 1772 07/12/2021 EMAIL 7/12/2021 These analytical results relate only to the sample identified in this report. Page 3 of 4 AX08486 Sample No. Method Test Description Results Qualifier SW846 8260C Bromoform < LOQ ug/L 0.50 05/18/2021 MG SW846 8260C Bromomethane < LOQ ug/L 0.50 05/18/2021 MG SW846 8260C Carbon tetrachloride < LOQ ug/L 0.50 05/18/2021 MG SW846 8260C Chlorobenzene < LOQ ug/L 0.50 05/18/2021